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Ammonium tartrate

Offer type: salePublished: 01.04.2015
Company:ChP Reaktiv-M
Seller:Mel'nik Maksim Vasil'evich
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Address:Ukraine, Zaporiz'ka Oblast', Zaporizhia
Ammonium tartrate. Properties:
White crystals of the monoclinic system, 1,601 square g/cm3. The reagent is soluble in water (6.3 g in 100 g of water at 15 °C). The air gradually loses NH3, turning into an acidic salt NH4HC4H4O6. Aqueous solutions moldy when the storage.
Preparation:
The drug is sufficiently high chemical purity is usually possible to obtain the cooperation of tartaric acid with ammonium carbonate.
Dissolve 90 g of tartaric acid H2C4H4O6 (h) in 100 ml of water at 50-60 °C and to the solution was added gradually (NH4)2CO3 (h. e. a., about 115 g) to a slightly alkaline reaction to phenolphthalein. The solution is boiled 20-30 min, evaporated on a water bath until the crystalline film, then quickly filtered and the filtrate cooled. The precipitated crystals are suctioned on a Buechner funnel and dried at 40 °C.
The output is ~85 g (~80%).